I like to make graphs.
I do. I’m not sure why, but I get an odd amount of enjoyment of plotting data out and seeing different relationships displayed graphically. I know, I know, there’s no hope for me. I’m reminded of the Simpson’s episode where Homer has suddenly become smart (I believe from having a crayon removed from his brain) and is finding himself rather sad. Lisa mentions that happiness and intelligence are often inversely correlated and says, “sigh... look, I made a graph of it.”
Anyhow, here’s one of my latest little ones :
During our experiments
it’s often necessary to keep track of the temperature
accurately. However, it’s often quite difficult to
get the conventional temperature measurement device,
the ubiquitous thermocouple, to function in our
system (usually it’s just impossible to use due to my
heavy reliance on RF induction heating). However, we
still need an accurate way to determine the
temperature both for our results and also so that we
don’t melt the crystals.
One of our standard tricks is to us the common piece
of knowledge that (most) things expand when heated.
Now, we can’t put calipers inside our chamber or do
anything like actually measuring the size difference
of these little crystals in the normal sense.
However, because we’re so often doing x-ray
scattering experiments, we are able to clearly
determine the average distance between the individual
atoms in the crystals. As the temperature increases
we are capable of seeing the distance between the
atoms change by a very tiny amount. The relation
between that expansion and temperature is well known.
So we just measure those distances periodically and
convert them to temperature. Now, it takes a little
time to do that and time is a precious quantity at a
light source. So we do it only when needed/reasonably
possible and then interpolate for places in between.
Above is that interpolation. The blue points are the
measured vales along with the accompanying
experimental uncertainty in each point. A red line is
then fit to those data points (I excluded the room
temperature-0 power data point as it looks like a
non-linear jump in temperature from the heater just
being turned on at its lowest power setting). So now
you can get the temperature for any power seeing to
within a very reasonable accuracy. We have to do that
each time we change samples or even whenever there’s
a large change in the sample position relative to the
heating coils, but that’s the price we pay. The
accuracy is much, much higher than the other
temperature measurement device easily available, a
pyrometer (which determines the temperature from the
light being emitted by the glowing crystal).
Ganesha
Here I’ve removed the
long hose from the front “snout,” but the effect is
still there. The two largest ports where the x-rays
come in and go out (which above are glass, but
replaced by Beryllium windows) make the eyes. It’s
got ears and a nose, along with a couple of dangling
arms/appendages. In truth it really was not intended
to look like something else. It’s a surface
scattering chamber complete with vacuum hardware and
measurement pieces, an RF induction heating system,
rotating sample stage feedthrough, fine-adjust gas
flow leak-valves, burst-disk, and enough windows that
I can see the sample positions during the experiment.
One of my friends took one look at it and said,
“Ganesh!” The name stuck. So we have
a vacuum chamber named after a Hindu deity.
Stranger things have happened (I recall the
himalayan pray flags that routinely went up during
experiments at one beamline at the ALS), but it is
a little odd to have my surface scattering
experiment refereed to with the proper name of a
god. “How is Ganesha today? Is Ganesha’s pressure
ok? Is Ganesha’s thermocouple measuring the
temperature accurately?”
It turns out that Ganesha the deity is often seen as
a patron of science (among many other things). So
perhaps the little vacuum chamber Ganesha is not
without some obtuse justification beyond mere
appearance. For better or worse, the name has stuck
and I surely hope that it’s not seen as offensive.
One further thought... Most of our samples involve at
least some (if not large) parts made from precious
metals such as gold and platinum. So there have ben
several occasions where such precious metals have
been “offered” to Ganesha. Thankfully he’s always
returned them to us intact.