I like to make graphs.
I do. I’m not sure why, but I get an odd amount of enjoyment of plotting data out and seeing different relationships displayed graphically. I know, I know, there’s no hope for me. I’m reminded of the Simpson’s episode where Homer has suddenly become smart (I believe from having a crayon removed from his brain) and is finding himself rather sad. Lisa mentions that happiness and intelligence are often inversely correlated and says, “sigh... look, I made a graph of it.”
Anyhow, here’s one of my latest little ones :
During our experiments
it’s often necessary to keep track of the temperature
accurately. However, it’s often quite difficult to
get the conventional temperature measurement device,
the ubiquitous thermocouple, to function in our
system (usually it’s just impossible to use due to my
heavy reliance on RF induction heating). However, we
still need an accurate way to determine the
temperature both for our results and also so that we
don’t melt the crystals.
One of our standard tricks is to us the common piece
of knowledge that (most) things expand when heated.
Now, we can’t put calipers inside our chamber or do
anything like actually measuring the size difference
of these little crystals in the normal sense.
However, because we’re so often doing x-ray
scattering experiments, we are able to clearly
determine the average distance between the individual
atoms in the crystals. As the temperature increases
we are capable of seeing the distance between the
atoms change by a very tiny amount. The relation
between that expansion and temperature is well known.
So we just measure those distances periodically and
convert them to temperature. Now, it takes a little
time to do that and time is a precious quantity at a
light source. So we do it only when needed/reasonably
possible and then interpolate for places in between.
Above is that interpolation. The blue points are the
measured vales along with the accompanying
experimental uncertainty in each point. A red line is
then fit to those data points (I excluded the room
temperature-0 power data point as it looks like a
non-linear jump in temperature from the heater just
being turned on at its lowest power setting). So now
you can get the temperature for any power seeing to
within a very reasonable accuracy. We have to do that
each time we change samples or even whenever there’s
a large change in the sample position relative to the
heating coils, but that’s the price we pay. The
accuracy is much, much higher than the other
temperature measurement device easily available, a
pyrometer (which determines the temperature from the
light being emitted by the glowing crystal).