I like to make graphs.
I do. I’m not sure why, but I get an odd amount of enjoyment of plotting data out and seeing different relationships displayed graphically. I know, I know, there’s no hope for me. I’m reminded of the Simpson’s episode where Homer has suddenly become smart (I believe from having a crayon removed from his brain) and is finding himself rather sad. Lisa mentions that happiness and intelligence are often inversely correlated and says, “sigh... look, I made a graph of it.”
Anyhow, here’s one of my latest little ones :
During our experiments it’s
often necessary to keep track of the temperature
accurately. However, it’s often quite difficult to get
the conventional temperature measurement device, the
ubiquitous thermocouple, to function in our system
(usually it’s just impossible to use due to my heavy
reliance on RF induction heating). However, we still
need an accurate way to determine the temperature both
for our results and also so that we don’t melt the
crystals.
One of our standard tricks is to us the common piece of
knowledge that (most) things expand when heated. Now,
we can’t put calipers inside our chamber or do anything
like actually measuring the size difference of these
little crystals in the normal sense. However, because
we’re so often doing x-ray scattering experiments, we
are able to clearly determine the average distance
between the individual atoms in the crystals. As the
temperature increases we are capable of seeing the
distance between the atoms change by a very tiny
amount. The relation between that expansion and
temperature is well known.
So we just measure those distances periodically and
convert them to temperature. Now, it takes a little
time to do that and time is a precious quantity at a
light source. So we do it only when needed/reasonably
possible and then interpolate for places in between.
Above is that interpolation. The blue points are the
measured vales along with the accompanying experimental
uncertainty in each point. A red line is then fit to
those data points (I excluded the room temperature-0
power data point as it looks like a non-linear jump in
temperature from the heater just being turned on at its
lowest power setting). So now you can get the
temperature for any power seeing to within a very
reasonable accuracy. We have to do that each time we
change samples or even whenever there’s a large change
in the sample position relative to the heating coils,
but that’s the price we pay. The accuracy is much, much
higher than the other temperature measurement device
easily available, a pyrometer (which determines the
temperature from the light being emitted by the glowing
crystal).
Ganesha
Here I’ve removed the long
hose from the front “snout,” but the effect is still
there. The two largest ports where the x-rays come in
and go out (which above are glass, but replaced by
Beryllium windows) make the eyes. It’s got ears and a
nose, along with a couple of dangling arms/appendages.
In truth it really was not intended to look like
something else. It’s a surface scattering chamber
complete with vacuum hardware and measurement pieces,
an RF induction heating system, rotating sample stage
feedthrough, fine-adjust gas flow leak-valves,
burst-disk, and enough windows that I can see the
sample positions during the experiment.
One of my friends took one look at it and said,
“Ganesh!” The name stuck. So we have a
vacuum chamber named after a Hindu deity. Stranger
things have happened (I recall the himalayan pray
flags that routinely went up during experiments at
one beamline at the ALS), but it is a little odd to
have my surface scattering experiment refereed to
with the proper name of a god. “How is Ganesha
today? Is Ganesha’s pressure ok? Is Ganesha’s
thermocouple measuring the temperature accurately?”
It turns out that Ganesha the deity is often seen as a
patron of science (among many other things). So perhaps
the little vacuum chamber Ganesha is not without some
obtuse justification beyond mere appearance. For better
or worse, the name has stuck and I surely hope that
it’s not seen as offensive.
One further thought... Most of our samples involve at
least some (if not large) parts made from precious
metals such as gold and platinum. So there have ben
several occasions where such precious metals have been
“offered” to Ganesha. Thankfully he’s always returned
them to us intact.